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Development and Validation of an Express Technique for Isolation and Quantitative Determination of Water-Soluble Polysaccharides from Roots of...

D’yakova N. A., Slivkin A. I., Samy'lina I. A., Gaponov S. P., Myndra A. A., Shushunova T. G.
Pharmaceutical Chemistry Journal
Vol.52, Issue4, P. 343-346
Опубликовано: 2018
Тип ресурса: Статья

DOI:10.1007/s11094-018-1819-0

Аннотация:
An express technique for isolation and quantitative determination of water-soluble polysaccharides from roots of Taraxacum officinaleWigg. was developed and allowed the assay time to be shortened to 3.5 h. The developed technique was validated for precision, accuracy, robustness, and linearity and was demonstrated to be precise under repeatable conditions, accurate, and robust. The precipitate mass was strictly linearly dependent on the analyzed raw-material mass for gravimetric determination of water-soluble polysaccharides from roots of T. officinale. The technique could be used for express quality control of T. officinale roots and for commercial production of inulin from this raw material. © 2018, Springer Science+Business Media, LLC, part of Springer Nature.
Ключевые слова:
Taraxacum officinale roots; Taraxacum officinale Wigg; water-soluble polysaccharides
polysaccharide; unclassified drug; water soluble polysaccharide; accuracy; Article; drug isolation; gravimetry; nonhuman; particle size; plant root; quality control; quantitative analysis; Taraxacum officinale; ultrasound assisted extraction
Язык текста: Английский
ISSN: 1573-9031
D’yakova N. A.
Slivkin A. I.
Samy'lina I. A. Irina Aleksandrovna 1943-
Gaponov S. P.
Myndra A. A.
Shushunova T. G.
Д’якова Н. А.
Сливкин А. И.
Самылина И. А. Ирина Александровна 1943-
Гапонов С. П.
Мyндра А. А.
Шушунова Т. Г.
Development and Validation of an Express Technique for Isolation and Quantitative Determination of Water-Soluble Polysaccharides from Roots of Taraxacum Officinale Wigg.
Development and Validation of an Express Technique for Isolation and Quantitative Determination of Water-Soluble Polysaccharides from Roots of...
Текст визуальный непосредственный
Pharmaceutical Chemistry Journal
Springer New York Consultants Bureau
Vol.52, Issue4 P. 343-346
2018
Статья
Taraxacum officinale roots Taraxacum officinale Wigg water-soluble polysaccharides
polysaccharide unclassified drug water soluble polysaccharide accuracy Article drug isolation gravimetry nonhuman particle size plant root quality control quantitative analysis Taraxacum officinale ultrasound assisted extraction
An express technique for isolation and quantitative determination of water-soluble polysaccharides from roots of Taraxacum officinaleWigg. was developed and allowed the assay time to be shortened to 3.5 h. The developed technique was validated for precision, accuracy, robustness, and linearity and was demonstrated to be precise under repeatable conditions, accurate, and robust. The precipitate mass was strictly linearly dependent on the analyzed raw-material mass for gravimetric determination of water-soluble polysaccharides from roots of T. officinale. The technique could be used for express quality control of T. officinale roots and for commercial production of inulin from this raw material. © 2018, Springer Science+Business Media, LLC, part of Springer Nature.